Buchi Rotavapo R-100 Manuel d'utilisateur

Rotavapor®R100OperationManual11593663en

2|Safety BÜCHILabortechnikAG10/60 OperationManualRotavapor®R100u Alwayswearappropriatepersonalprotectiveequipmentsuchassafetygoggles,

BÜCHILabortechnikAG Productdescription|3OperationManualRotavapor®R100 11/603 Productdescription3.1 DescriptionoffunctionTheRotavapor®R1

3|Productdescription BÜCHILabortechnikAG12/60 OperationManualRotavapor®R1003.2 Configuration3.2.1 Frontview13Fig.1:ConfigurationofR100

BÜCHILabortechnikAG Productdescription|3OperationManualRotavapor®R100 13/603.2.2 RearviewFig.3:Rearview R1001 Powersupplyconnection 3

3|Productdescription BÜCHILabortechnikAG14/60 OperationManualRotavapor®R1003.2.4 TypicalapplicationInordertousetheRotavapor®R100tob

BÜCHILabortechnikAG Productdescription|3OperationManualRotavapor®R100 15/603.2.5 TypeplateThetypeplateisontherighthandsideoftheRo

3|Productdescription BÜCHILabortechnikAG16/60 OperationManualRotavapor®R1003.2.6 WarningsymbolsonthedeviceThedevicecarriesthefollowin

BÜCHILabortechnikAG Productdescription|3OperationManualRotavapor®R100 17/603.4 Technicaldata3.4.1 Rotavapor®R100Dimensions(WxHxD) 617

3|Productdescription BÜCHILabortechnikAG18/60 OperationManualRotavapor®R1003.4.3 AmbientconditionsMax.altitudeabovesealevel 2000mAmbien

BÜCHILabortechnikAG Productdescription|3OperationManualRotavapor®R100 19/603.5 Safetyfeatures3.5.1 OverheatcutoutToprotectagainstoverhe

ImprintProductIdentification:OperationManual(Original)Rotavapor®R10011593663enPublicationdate:12.2014,VersionBBÜCHILabortechnikAGMeiersegg

4|Transportandstorage BÜCHILabortechnikAG20/60 OperationManualRotavapor®R1004 Transportandstorage4.1 TransportIMPORTANTRiskofbreakagedu

BÜCHILabortechnikAG Installation|5OperationManualRotavapor®R100 21/605 Installation5.1 InstallationsiteTheinstallationsitemustmeetthefo

5|Installation BÜCHILabortechnikAG22/60 OperationManualRotavapor®R1005.3 Fittingthevaporductandcondenser14322u Insertvaporduct(4)into

BÜCHILabortechnikAG Installation|5OperationManualRotavapor®R100 23/605.4 FittingtheglassstopcockMaterialsrequired: GreaseGlisseal40blu

5|Installation BÜCHILabortechnikAG24/60 OperationManualRotavapor®R1005.5 ConnectingthevacuumandcoolingmediatubingToachieveoptimumdist

BÜCHILabortechnikAG Installation|5OperationManualRotavapor®R100 25/605.6 Electricalconnectionsu Makesurethattheavailablepowersupplymat

5|Installation BÜCHILabortechnikAG26/60 OperationManualRotavapor®R1005.8 Settingupandfillingtheheatingbath12u Locatetheheatingbath(1

BÜCHILabortechnikAG Operation|6OperationManualRotavapor®R100 27/606 Operation6.1 Preparations6.1.1 PreparingtheheatingbathCAUTIONRiskofs

6|Operation BÜCHILabortechnikAG28/60 OperationManualRotavapor®R1006.1.2 FittingtheevaporatingflaskIMPORTANTRiskofevaporatingflaskdamage

BÜCHILabortechnikAG Operation|6OperationManualRotavapor®R100 29/606.1.3 Adjustingimmersionangleofevaporatingflasku SwitchofftheRotavap

BÜCHILabortechnikAG ContentsOperationManualRotavapor®R100 iiiContents1 Aboutthisdocument...

6|Operation BÜCHILabortechnikAG30/60 OperationManualRotavapor®R1006.1.4 FittingthereceivingflaskMaterialsrequired: GreaseGlisseal40blu

BÜCHILabortechnikAG Operation|6OperationManualRotavapor®R100 31/60Movingtheverticaladjustmentrangeup/downCAUTIONRiskofinjurywhenadju

6|Operation BÜCHILabortechnikAG32/60 OperationManualRotavapor®R1006.2 PerformingdistillationDANGERRiskofpoisoningfrominhalationofhazar

BÜCHILabortechnikAG Operation|6OperationManualRotavapor®R100 33/60u Immersetheevaporatingflaskintheheatingbath(seeChapter6.2.1"

6|Operation BÜCHILabortechnikAG34/60 OperationManualRotavapor®R1006.2.2 AdjustingdistillationconditionsToobtainoptimumdistillationcondit

BÜCHILabortechnikAG Operation|6OperationManualRotavapor®R100 35/606.2.3 OptimizationdistillationDependingonthesolventinvolved,itmayals

6|Operation BÜCHILabortechnikAG36/60 OperationManualRotavapor®R100u Inapplicationswherenovacuumisapplied,lowerthetemperatureoftheh

BÜCHILabortechnikAG Operation|6OperationManualRotavapor®R100 37/606.3 Finishingdistillationu Raisetherotarydriveunit(seeChapter6.2.1&

6|Operation BÜCHILabortechnikAG38/60 OperationManualRotavapor®R1006.3.2 Removingthereceivingflasku Raisetherotarydriveunit(seeChapter

BÜCHILabortechnikAG Cleaningandservicing|7OperationManualRotavapor®R100 39/607 CleaningandservicingNOTEUsersmayonlycarryouttheservic

Contents BÜCHILabortechnikAGiv OperationManualRotavapor®R1005 Installation...

7|Cleaningandservicing BÜCHILabortechnikAG40/60 OperationManualRotavapor®R1007.3 CheckingsealsSealsarewearparts.Theyhavetoberegular

BÜCHILabortechnikAG Cleaningandservicing|7OperationManualRotavapor®R100 41/607.5 CleaningtheheatingbathIMPORTANTRiskofshortcircuitfro

8|Helpwithfaults BÜCHILabortechnikAG42/60 OperationManualRotavapor®R1008 Helpwithfaults8.1 Faults,possiblecausesandremediesFault Possi

BÜCHILabortechnikAG Helpwithfaults|8OperationManualRotavapor®R100 43/60Fault Possiblecause RemedyOptimumdistillationnotachievedToomuch

8|Helpwithfaults BÜCHILabortechnikAG44/60 OperationManualRotavapor®R1008.2 Remedy8.2.1 ResettingoverheatsafetycutoutCAUTIONRiskofskin

BÜCHILabortechnikAG Helpwithfaults|8OperationManualRotavapor®R100 45/608.2.2 ReplacingthefuseThefuseisontherearoftheheatingbath.u

9|Takingoutofserviceanddisposal BÜCHILabortechnikAG46/60 OperationManualRotavapor®R1009 Takingoutofserviceanddisposal9.1 Takingout

BÜCHILabortechnikAG Appendix|10OperationManualRotavapor®R100 47/6010 Appendix10.1 SolventtableSolvent Formula Molarmassing/molEvaporatione

10|Appendix BÜCHILabortechnikAG48/60 OperationManualRotavapor®R100Solvent Formula Molarmassing/molEvaporationenergyinJ/gBoilingpointin

BÜCHILabortechnikAG Appendix|10OperationManualRotavapor®R100 49/6010.2.1 GlassapparatusV040627 000646040625023875023900028096 02860600063604

BÜCHILabortechnikAG Aboutthisdocument|1OperationManualRotavapor®R100 5/601 AboutthisdocumentTheseoperatinginstructionsdescribetheRota

10|Appendix BÜCHILabortechnikAG50/60 OperationManualRotavapor®R10010.2.2 GlassapparatusC040627 000646023875 023900 0280960320130006360286060

BÜCHILabortechnikAG Appendix|10OperationManualRotavapor®R100 51/6010.2.3 AccessoriesHeatingBathHeatingBathB100.2095°C,220240VHeatingp

10|Appendix BÜCHILabortechnikAG52/60 OperationManualRotavapor®R100Waterregulationnozzle.Restrictionvalve,hoseclamp,sieveUsedwhentapw

BÜCHILabortechnikAG Appendix|10OperationManualRotavapor®R100 53/60Glass,SJ24/40,2000mL 008765Glass,SJ24/40,2000mL,P+G 025262Glass,SJ24/4

10|Appendix BÜCHILabortechnikAG54/60 OperationManualRotavapor®R100Glass,SJ29/32,1500mL,forevaporation 034230Glass,SJ29/32,500mL,fordry

BÜCHILabortechnikAG Appendix|10OperationManualRotavapor®R100 55/60Glass,SJ24/40,incl.20mLzyl.flask(20pcs) 011578Glass,SJ24/40,incl.50

10|Appendix BÜCHILabortechnikAG56/60 OperationManualRotavapor®R100Capnuts,set.10pcs,capnutswithhole,GL14 04195610.2.5 SparepartsDrain

BÜCHILabortechnikAG Appendix|10OperationManualRotavapor®R100 57/6010.3 ListofabbreviationsAbbreviation MeaningADR Accordeuropéenrelatifau

10|Appendix BÜCHILabortechnikAG58/60 OperationManualRotavapor®R10010.5 HealthandsafetyDeclarationregardingthesafety,hazardsandsafedis

1|Aboutthisdocument BÜCHILabortechnikAG6/60 OperationManualRotavapor®R100Symbol Meaning Symbol MeaningHotsurface Healthharmingorirritant

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BÜCHILabortechnikAG Safety|2OperationManualRotavapor®R100 7/602 Safety2.1 IntendeduseTheRotavapor®R100isintendedforevaporatingandcon

2|Safety BÜCHILabortechnikAG8/60 OperationManualRotavapor®R1002.3 StaffqualificationUnqualifiedpersonsareunabletoidentifyrisksandare

BÜCHILabortechnikAG Safety|2OperationManualRotavapor®R100 9/602.4.2 HighinternalpressureTheevaporationoffluidscanproducehighpressures